Color study of historic silks
Abstract
The chemical characterization of silk textiles of historic value may be necessary to achieve a better understanding of the production processes applied, to evaluate their preservation, to detect manipulations or forgeries, and to value the combination of tradition and innovation in contemporary manufacturing techniques. The main objective of this work was to study four historical silks from the Garín collection, all of them from the 20th century, although with 19th century designs. To this end, non-invasive spectroscopic and microscopy techniques were applied in order to obtain information on the dyes used during their production and their link with those used in the silk industry in previous centuries, and to ascertain their state of conservation. Moreover, the images in LM, SEM and CM are contributing to the development of a 3D virtual loom that will favor more accessible and inclusive museography in museums specialized in the silk sector. Both the study of dyes and silk fibers and their virtual reproduction through artificial intelligence programs applied to the study of cultural heritage, by specialists from the Robotics Institute of the Universitat de València, has been developed in the framework of the SILKNOW project (https://silknow.eu/).
Downloads
References
AHMED, H. E., DARWISH, S. S. (2012). “Effect of museum conditions on historical dyed silk fabric with madder dye”, Journal of Polymers and the Environment, 20: 596-606. https://doi.org/10.1007/s10924-012-0421-x.
AL-SHARAIRI, N., SANDU, I. C. A., VASILACHE, V., SANDU, I. (2020). “Recognition of natural silk fibers, dyes and metal threads of historical Romanian textile fragments using the multi-analytical techniques approach”. Textile Research Journal, 90 (15-16): 1671-1688. https://doi.org/10.1177/0040517519898827.
BADILLO-SANCHEZ, D., CHELAZZI, D., GIORGI, R., CINCINELLI, A., BAGLIONI, P. (2019). “Understanding the structural degradation of South American historical silk: a focal plane array (FPA) FTIR and multivariate analysis”. Scientific Reports, 9: 17239. https://doi.org/10.1038/s41598-019-53763-5.
BARBACHE, S., LAMHASNI, T., EL BAKKALI, A., LYAZIDI, S. A., HADDAD, M., BEN-NCER, A., HNACH, M. (2018). “Optical analyses of wool dyeing materials in ancient Moroccan carpets “Zarbia(s)”: combination of UV-Vis diffuse reflectance, 3D-fluorescence and raman spectroscopies”. Dyes and Pigments, 153: 256-265. https://doi.org/10.1016/j.dyepig.2018.02.033.
BOULET-AUDET, M., VOLLRATH, F., HOLLAND, C. (2015). “Identification and classification of silks using infrared spectroscopy”. Journal of Experimental Biology, 218: 3138-3149. https://doi.org/10.1242/jeb.128306.
DE FERRI, L., TRIPODI, R., MARTIGNON, A., FERRARI, E. S., LAGRUTTA-DÍAZ, A. C., VALLOT-TO, D., POJANA G. (2018). “Non-invasive study of natural dyes on historical textiles from the collection of Michelangelo Guggenheim”. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 204: 548-567. https://doi.org/10.1016/j.saa.2018.06.026.
DING, L., GONG, T., WANG, B., YANG, Q., LIU, W., PEMO, R., METOK, T. (2021). “Non-invasive study of natural dyes in textiles of the Qing Dynasty using fiber optic reflectance spectroscopy”. Journal of Cul-tural Heritage, 47: 69-78. https://doi.org/10.1016/j.culher.2020.10.013.
FONSECA, B., PATTERSON, C. S., GANIO, M., MACLENNAN, D., TRENTELMAN, K. (2019). “Seeing red: towards an improved protocol for the identification of madder and cochineal-based pigments by fiber optics reflectance spectroscopy (FORS)”. Heritage Science, 7: 92. https://doi.org/10.1186/s40494-019-0335-1.
GAITAN, M., ALBA, E. LEÓN, A., PÉREZ, M. SEVILLA, J., PORTALES, C. (2019). “Towards the Preservation and Dissemination of Historical Silk Weaving Techniques in the Digital Era”. Heritage 2 (3), 1892-1911; https://doi.org/10.3390/heritage2030115
GULMINI, M., IDONE, A., DIANA, E., GASTALDI, D., VAUDAN, D., ACETO, M. (2013). “Identification of dyestuffs in historical textiles: strong and weak points of a non-invasive approach”. Dyes and Pigments, 98: 136-145. https://doi.org/10.1016/j.dyepig.2013.02.010.
HACKE , M. (2008). Weighted silk: history, analysis and conservation. Studies in Conservation, 53 (2): 3-15, https://doi.org/10.1179/sic.2008.53.Supplement-2.3
HAN, J., WANROOIJ, J., VAN BOMMEL, M., QUYE, A. (2017). “Characterization of chemical components for identifying historical Chinese textile dyes by ultra high performance liquid chromatography-photodiode array electrospray ionisation mass spectrometry”. Journal of Chromatography A, 1479: 87-96. http://dx.doi.org/10.1016/j.chroma.2016.11.044.
KAPLAN, D., WADE ADAMS, W., FARMER, B. and VINEY C. (1994). "Silk: Biology, structure, properties and genetics", en D. Kaplan, W. W. Adams, B. Farmer y C. Viney (eds.), Silk Polymers: Materials Science and Biotechnology, Washington D.C., ACs Publications, 2–16.
KIM, S., SEONG, H., HER, Y., CHUN, J. (2019). “A study of the development and improvement of fashion products using a FDM type 3D printer”. Fash Text 6, 9. https://doi.org/10.1186/s40691-018-0162-0
KOPERSKA, M., ŁOJEWSKI, T., ŁOJEWSKA, J. (2011). “Vibrational spectroscopy to study degradation of natural dyes. Assessment of oxygen-free cassette for safe exposition of artefacts”. Analytical and Bioanalytical Chemistry, 399: 3271-3283.
KRAMELL, A. E., GARCÍA-ALTARES, M., PÖTSCH, M., KLUGE, R., ROTHER, A., HAUSE, G., HERTWECK, C., CSUK, R. (2019). “Mapping natural dyes in archaeological textiles by imaging mass spec-trometry”. Scientific Reports, 9: 2331. https://doi.org/10.1038/s41598-019-38706-4.
MA, M., HUSSAIN, M., DONG, S., ZHOU, W. (2016). “Characterization of the pigment in naturally yellow-colored domestic silk”. Dyes and Pigments, 124: 6-11. http://dx.doi.org/10.1016/j.dyepig.2015.08.003.
MIKOLAYCHUK, E., PINYAGNA, N. (1997). “Silk as a textile material, reasons of destruction”, en stf Jubilee Conference: Silk. Different Aspects, Estocolmo, Urram, s/f.
MILLER, J.E., REAGAN, B.M. (1989). "Degradation in weighted and unweighted historic silks". Journal of the American Institute for Conservation 28 (2): 97–115.
MILLINGTON, K. R. (2012). “Diffuse reflectance of fibrous proteins”. Amino Acids, 43: 1277-1285. https://doi.org /10.1007/s00726-011-1201-y.
MOINI, M., ROLLMAN, C. M. (2017). “Buyid silk and the tale of Bibi Shahrbanu: identification of biomarkers of artificial aging (forgery) of silk”. Analytical Chemistry, 89: 10158-10161. https://doi.org/10.1021/acs.analchem.7b02854.
PETROVICIU, I., TEODORESCU, I., ALBU, F., VIRGOLICI, M., NAGODA, E., MEDVEDOVICI A. (2019). “Dyes and biological sources in nineteenth to twentieth century ethnographic textiles from Transylvania, Romania”. Heritage Science, 7: 15. https://doi.org/10.1186/s40494-019-0255-0.
POTTIER, F., MICHELIN, A., KWIMANG, S., ANDRAUD, C., GOUBARD, F., LAVÉDRINE, B. (2019). “Macroscopic reflectance spectral imaging to reveal multiple and complementary types of information for the non-invasive study of an entire polychromatic manuscript”. Journal of Cultural Heritage, 35: 1-15. https://doi.org/10.1016/j.culher.2018.06.001.
SHAHID, M., WERTZ, J., DEGANO, I., ACETO, M., KHAN, M. I., QUYE, A. (2019). “Analytical methods for determination of anthraquinone dyes in historical textiles: a review”. Analytica Chimica Acta, 1083: 58-87. https://doi.org/10.1016/j.aca.2019.07.009
TAMBURINI, D., DYER, J., DAVIT, P., ACETO, M., TURINA, V., BORLA, M., VENDENBEUSCH, M., GULMINE, M. (2019a). “Compositional and micromorphological characterization of red colorants in ar-chaeological textiles from pharaonic Egypt”. Molecules, 24: 3761. https://www.mdpi.com/1420-3049/24/20/3761.
TAMBURINI, D., CARTWRIGHT, C. R., PULLAN, M., VICKERS, H. (2019b). “An investigation of the dye palette in Chinese silk embroidery from Dunhuang (Tang dynasty)”. Archaeological and Anthropological Sciences, 11: 1221-1239. https://doi.org/10.1007/s12520-017-0592-4.
TAMBURINI, D., DYER, J. (2019). “Fiber optic reflectance spectroscopy and multispectral imaging for the non-invasive invstigation of Asian colourants in Chinese textiles from Dunhuang (7th-10th century AD)”. Dyes and Pigments, 162: 494-511. https://doi.org/10.1016/j.dyepig.2018.10.054.
TAMBURINI, D. (2019). “Investigating Asian colourants in Chinese textiles from Dunhuang (7th-10th Centu-ry AD) by high performance liquid chromatography tandem mass spectrometry – Towards the creation of a mass spectra database. Dyes and Pigments, 163: 454-474. https://doi.org/10.1016/j.dyepig.2018.12.025.
VERHECKEN, A., STORME, P., SCHALM, O. (2014). “UV-Vis reflectance spectrometry study of the dyed silks in a relic shrine found in Antwerp, Belgium”. e-Preservation Science, 11: 99-104.
- Copyright and intellectual property belongs to author. Author guarantees editing and publishing rights to Ge-Conservación Journal, under a Creative Commons Attribution License. This license allows others to share the work with authorship and the original source of publication acknowledgement.
- Articles can be used for scientific and educational purposes but never for commercial use, being sanctioned by law.
- The whole content of the article is author’s responsibility.
- Ge-Conservación Journal and authors may establish additional agreements for non-exclusive distribution of the work version published at the Journal (for example, on institutional repositories or on a book) with acknowledgment of the original publication on this Journal.
- Author is allowed and encouraged to disseminate his works electronically (for example, on institutional repositories or on its own website) after being published on Ge-Conservación Journal. This will contribute for fruitful interchanges as also for wider and earlier citations of the author’s works.
- Author’s personal data will only be used for the Journal purposes and will not be given to others.